Back to Article
Microwave Assisted Synthesis of 3, 5-Disubstituted 1, 2, 4-Triazole Based Piperazine Amide and Urea Derivatives
Online Journal of Chemistry
| Vol 1, Issue 1
Table 2. Results of the reaction ofnitrile with hydrazide under different conditions.
| Temp (°C) | Yield (%) | Temp (°C) | Yield (%) | ||
| 1. | Ethanol | 90 | - | 90 | 20 |
| 2. | Butanol | 90 | 10 | 90 | 40 |
| 3. | Tert-butanol | 90 | 25 | 90 | 50 |
| 4. | Xylene | 120 | 30 | 120 | 60 |
| 5. | DMF | 120 | 50 | 120 | 92 |
| 6. | DMSO | 150 | 40 | 150 | 75 |